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Biomechanical aspects of the reconstruction of the acetabulum
Slávik, Ondrej ; Marcián, Petr (referee) ; Florian, Zdeněk (advisor)
The research part of bacelor’s thesis Biomechanical aspects of the reconstruction of the acetabulum is dealing with historical development and current methods of solving the issue of pathological hip joints in case when use of total endoprosthesis is not suitable, for example in children. Also the anatomical view, related to the given problem situation, is outlined and the most significant disorders of the hip joint, which are connected with these cases, are characterized. In the practical part of this work, there are results of the analysis model between pathological and physiological hips analyzed and qualitatively compared, followed by the solution of the concact forces in these two situations.
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Processing and properties of transparent polycrystalline ceramic materials
Tásler, Jan ; Pouchlý, Václav (referee) ; Maca, Karel (advisor)
The presented diploma thesis is focused on the preparation and properties of transparent polycrystalline ceramic materials based on Al2O3. Theoretically, the most important technological aspects of the processing of these materials are presented. Detailed attention is given to transparent Al2O3 polycrystalline ceramics doped with rare earth elements. The influence of microstructural parameters on the optical properties (represented by RIT) is investigated on Al2O3 samples doped and codoped with dysprosium, terbium and chromium. A significant effect of the average grain size on the light transmittance of all samples is observed. The highest RIT = 55 % (measured by a laser beam with a wavelength of 632,8 nm) was achieved by an optimized preparation process for a sample doped with 0,05 at. % of dysprosium. For all samples photoluminescent properties are also analysed. The photoluminescent emission spectra correspond to the activation of doping elements. In case of the terbium and chromium codoped samples, the differences in the activation of individual dopants depending on different excitation wavelengths were demonstrated, resulting in different colour emissions for different excitation wavelengths.
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Production of the “ Hauling lug pawl“ component
Jansa, Slavomír ; Ohnišťová, Petra (referee) ; Žák, Ladislav (advisor)
This magister thesis focuses on possibilities of replacement of milled Hauling lug pawl by cheaper component made by MIM technology with additional chemical-thermal treatment. Two thirds of costs should be saved if application is fruitful. Despite huge mix of combinations of steel ASTM-A29-AISI 8620, ASTM-A29-AISI 4140 and chemical-thermal treatment, no combination was successful. Several series of samples have been created but not even the use of HIP and ARCOR technology helped to pass circuit breaker storage life tests. Successful application of MIM technology would require additional design changes or choice of different suitable part.
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Transparent polycrystalline ceramic materials with cubic lattice structure
Kučera, Jan ; Pouchlý, Václav (referee) ; Maca, Karel (advisor)
The presented work is focused on the study of the influence of preparation parameters on the optical properties of polycrystalline cubic ZrO2 (stabilized with 8 mol.% Y2O3). Furthermore, the work deals with the doping of c-ZrO2 with TiO2 and its effect on the luminescence properties of ZrO2. The examined samples were prepared by uniaxial pressing (10 MPa), followed by a cold isostatic pressing (300 and 700 MPa), pressureless sintering (1340–1380 °C, 10 min), and hot isostatic pressing (1200–1400 °C, 4 h, 200 MPa). In this work, it is shown that the optical properties are significantly affected by the temperature of the hot isostatic pressing, the thickness of the sample, and also by the wavelength of the incident light. A maximum real in-line transmission of 68.8 % was achieved, which is 90.5 % of the theoretical limit for c-ZrO2 at an incident radiation wavelength of 632.8 nm. A low-pressure infiltration method and a powder mixing method were used to prepare the doped ZrO2 ceramic sample. With doping, the maximum of the excitation spectrum shifted from 295 nm (4.20 eV) for the undoped ZrO2 to 320 nm (3.87 eV) for the doped samples. Doping led to an increase in emission intensity compared to a pure ZrO2 by up to 23 times. The maximum emission intensity at 545 nm wavelength was achieved for samples doped by infiltration method with a nominal 0.1 mol.% TiO2 content.
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Processing of compact polycrystalline YAG ceramics
Kaplan, Lukáš ; Pouchlý, Václav (referee) ; Kachlík, Martin (advisor)
In the literary part of this master thesis a research on various methods of preparation of dense polycrystalline YAG ceramics and the effects of sintering on the densification and other desired properties of such prepared YAG ceramics was carried out, the transparency after addition of dopant elements was also discussed. In the experimental part of the thesis, samples of dense polycrystalline YAG ceramics were prepared by SSR method and the effect of sintering on the densification and porosity of the YAG ceramic samples was studied. Relative density, porosity, phase purity and transparency were measured on the sintered samples. These measurements were compared with the results of the works reported in the literature section.
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Transparent ceramic materials
Krupa, Filip ; Drdlík, Daniel (referee) ; Maca, Karel (advisor)
This Bachelor thesis deals with processing of transparent cubic ZrO2 ceramic doped by 8 mol% Y2O3. Technology used in this Bachelor thesis are uniaxial pressing, cold isosatic pressing, SPS and hot isostatic pressing. Microstructure, real in-line transparency and hardness were evaluated for sintered transparent materials.
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Ceramic materials based on spinel MgAl2O4 for optical applications
Rychnovský, Daniel ; Maca, Karel (referee) ; Drdlík, Daniel (advisor)
This diploma thesis deals with preparation of transparent ceramics based on spinel MgAl2O4 and effect of Cr3+, Tb3+ doping on optical properties. Preparation of samples was optimized using several ways to prepare non-defect ceramic samples with the highest relative density of green body. The final step of the processing included hot isostatic pressing resulting in transparent undoped and doped spinel ceramics. The highest values of RIT (real in- line transmittance) of undoped and doped samples were measured between 77–79 %. It was found by measuring photoluminescence properties of prepared samples that increasing concentration of Cr3+ resulted to higher peak intensities. The most intense emission peak was measured in red spectral area at wavelength of 685 nm. In the case of Tb3+-doped spinel, the maximum peak intensities were measured at concentration of 0.075 at. % and the most intense emission peak was measured in green spectral area at wavelength of 545 nm.
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Production of the “ Hauling lug pawl“ component
Jansa, Slavomír ; Ohnišťová, Petra (referee) ; Žák, Ladislav (advisor)
This magister thesis focuses on possibilities of replacement of milled Hauling lug pawl by cheaper component made by MIM technology with additional chemical-thermal treatment. Two thirds of costs should be saved if application is fruitful. Despite huge mix of combinations of steel ASTM-A29-AISI 8620, ASTM-A29-AISI 4140 and chemical-thermal treatment, no combination was successful. Several series of samples have been created but not even the use of HIP and ARCOR technology helped to pass circuit breaker storage life tests. Successful application of MIM technology would require additional design changes or choice of different suitable part.
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